Nevşehir Hacı Bektaş Veli University Course Catalogue
|
|||||
| Year/Semester of Study | 1 / Fall Semester | ||||
| Level of Course | 2nd Cycle Degree Programme | ||||
| Type of Course | Optional | ||||
| Department | CHEMISTRY (MASTER'S DEGREE) | ||||
| Pre-requisities and Co-requisites | None | ||||
| Mode of Delivery | Face to Face | ||||
| Teaching Period | 14 Weeks | ||||
| Name of Lecturer | HİLAL İNCEBAY (hincebay@nevsehir.edu.tr) | ||||
| Name of Lecturer(s) | |||||
| Language of Instruction | Turkish | ||||
| Work Placement(s) | None | ||||
| Objectives of the Course | |||||
| The characterization of polymers, giving detailed information about the various purification techniques, characterization techniques and properties of the final product is intended to examine. | |||||
| Learning Outcomes | PO | MME | |
| The students who succeeded in this course: | |||
| LO-1 | Learn the methods of characterizing polymers |
PO-1 Upon successful completion of this programme, graduate students will: Have advance knowledge and skills in the area of specialized.
PO-2 Do enough practical and theoretical advance studies. PO-3 Evaluate the scientific data obtained from advance studies and present scientific results. PO-4 Defend the thesis that in the front of a jury composed by experts. PO-5 Follow the literature in the area of specialized. |
Examination |
| PO: Programme Outcomes MME:Method of measurement & Evaluation |
|||
| Course Contents | ||
| Characterization techniques, polymers, molecular mass, molecular mass distribution and the determination methods: end group analysis, Colligative properties, light scattering, diffusion, ultracentrifugation, sedimentation equilibrium and sedimantsyon speed, viscometer and GPC methods. Thermal characterization of polymers, DTA, DSC, TGA. Dynamic mechanical thermal analysis. Dynamic light scattering | ||
| Weekly Course Content | ||
| Week | Subject | Learning Activities and Teaching Methods |
| 1 | Introduction: Characterization place in science and industry, the importance of polymers, an overview of characterization techniques. | evaluation methods |
| 2 | Polymers fractionation techniques: vacuum technique, freeze drying technique, selective precipitation technique, | evaluation methods |
| 3 | Molecular weight determination methods: viscosity, | evaluation methods |
| 4 | Molecular weight determination methods: end group analysis, | evaluation methods |
| 5 | Molecular weight determination methods: Colligative features | evaluation methods |
| 6 | Molecular weight determination methods: ultrasantrfüj | evaluation methods |
| 7 | Molecular weight determination methods: Gel Permeation Chromatography (GPC) and high-pressure gel permeation chromatography | evaluation methods |
| 8 | mid-term exam | |
| 9 | Molecular weight determination methods: static light scattering: zimmi plot, the Debye plot, girasyon radius, times the number of secondary spin, theta temperature, micelle formation, critical micelle concentration and temperature | evaluation methods |
| 10 | Molecular weight determination methods: static light scattering: static light scattering data and hydrodynamic parameters in determining the use of polymerization termodinamiğinde | evaluation methods |
| 11 | Thermal Characterization: Thermal transitions and factors affecting them, differential thermal analysis, DTA, Thermal Characterization of differential scanning calorimeter, DSC, thermomechanical analysis, TMA, | evaluation methods |
| 12 | Thermal Characterization: Thermogravimetric methods, thermogravimetric analysis | evaluation methods |
| 13 | Pyrolysis-gas chromatography (PGC), yanabilirlika, and mechanisms of thermal decomposition reactions, and preparation of heat-resistant polymers | evaluation methods |
| 14 | Dynamic light scattering (DLS) method of determination of the hydrodynamic properties of polymers. | evaluation methods |
| 15 | Dynamic light scattering (DLS) method of determination of the hydrodynamic properties of polymers. | evaluation methods |
| 16 | final exam | |
| Recommend Course Book / Supplementary Book/Reading | ||
| 1 | 1) Polymer Chemistry, Professor. Dr. Mehmet EAVES, Gazi Publications, 2004, 2) Polymer characterization, Hunt and James, Blackie Academic and Professional, London, 1993, 3) Polymer Spectroscopy, Allan H. Fawcett, John Wiley and Sons, NY, 1997. | |
| Required Course instruments and materials | ||
| projection tool | ||
| Assessment Methods | |||
| Type of Assessment | Week | Hours | Weight(%) |
| mid-term exam | 7 | 2 | 40 |
| Other assessment methods | |||
| 1.Oral Examination | |||
| 2.Quiz | |||
| 3.Laboratory exam | |||
| 4.Presentation | |||
| 5.Report | |||
| 6.Workshop | |||
| 7.Performance Project | |||
| 8.Term Paper | |||
| 9.Project | |||
| final exam | 15 | 2 | 60 |
| Student Work Load | |||
| Type of Work | Weekly Hours | Number of Weeks | Work Load |
| Weekly Course Hours (Theoretical+Practice) | 3 | 13 | 39 |
| Outside Class | |||
| a) Reading | 4 | 12 | 48 |
| b) Search in internet/Library | 5 | 14 | 70 |
| c) Performance Project | 1 | 1 | 1 |
| d) Prepare a workshop/Presentation/Report | 0 | ||
| e) Term paper/Project | 0 | ||
| Oral Examination | 0 | ||
| Quiz | 0 | ||
| Laboratory exam | 0 | ||
| Own study for mid-term exam | 10 | 1 | 10 |
| mid-term exam | 1 | 1 | 1 |
| Own study for final exam | 10 | 1 | 10 |
| final exam | 1 | 1 | 1 |
| 0 | |||
| 0 | |||
| Total work load; | 180 | ||