Nevşehir Hacı Bektaş Veli University Course Catalogue

Information Of Programmes

INSTITUTE OF SCIENCE / NBT504 - NANOBİLİM VE NANOTEKNOLOJİ ANABİLİM DALI

Code: NBT504 Course Title: SOL-GEL PROCESS Theoretical+Practice: 3+0 ECTS: 6
Year/Semester of Study 1 / Spring Semester
Level of Course 2nd Cycle Degree Programme
Type of Course Optional
Department NANOBİLİM VE NANOTEKNOLOJİ ANABİLİM DALI
Pre-requisities and Co-requisites None
Mode of Delivery Face to Face
Teaching Period 14 Weeks
Name of Lecturer FATMA ZEHRA KOÇAK (fzkocak@nevsehir.edu.tr)
Name of Lecturer(s)
Language of Instruction Turkish
Work Placement(s) None
Objectives of the Course
To understand the sol-gel technique and its steps. Learning the concepts effective in the sol-gel technique. It is aimed to make students understand the application areas. Characterization of materials and understanding structure-property relationships in materials

Learning Outcomes PO MME
The students who succeeded in this course:
LO-1 Explain sol and gel terms PO-1 Students will get information by doing research in the field of Engineering, evaluate the information, interpret and apply.
PO-2 Students complete information and apply the scientific method; It integrates the knowledge of different disciplines.
PO-3 Students fictions engineering problems, develop methods to solve and apply innovative methods in solution.
PO-6 Students develop methods to solve a defined problem and apply innovative methods in technology solutions.
PO-8 Students will observe the social, scientific and ethical values.
Examination
Presentation
Performance Project
LO-2 can explain the sol-gel synthesis reactions PO-1 Students will get information by doing research in the field of Engineering, evaluate the information, interpret and apply.
PO-2 Students complete information and apply the scientific method; It integrates the knowledge of different disciplines.
PO-3 Students fictions engineering problems, develop methods to solve and apply innovative methods in solution.
PO-6 Students develop methods to solve a defined problem and apply innovative methods in technology solutions.
Examination
Presentation
Performance Project
LO-3 can explain the properties and applications of sol-gel based materials PO-1 Students will get information by doing research in the field of Engineering, evaluate the information, interpret and apply.
PO-2 Students complete information and apply the scientific method; It integrates the knowledge of different disciplines.
PO-3 Students fictions engineering problems, develop methods to solve and apply innovative methods in solution.
PO-5 Students are aware of new and emerging practice of the profession, examine them and learn when necessary.
PO-6 Students develop methods to solve a defined problem and apply innovative methods in technology solutions.
Examination
Presentation
Performance Project
LO-4 can learn the characterization techniques and interperate the structure and property relationships PO-1 Students will get information by doing research in the field of Engineering, evaluate the information, interpret and apply.
PO-3 Students fictions engineering problems, develop methods to solve and apply innovative methods in solution.
PO-5 Students are aware of new and emerging practice of the profession, examine them and learn when necessary.
PO-7 Students will share their work process and the results in writing or verbally.
PO-8 Students will observe the social, scientific and ethical values.
Examination
Presentation
Performance Project
PO: Programme Outcomes
MME:Method of measurement & Evaluation

Course Contents
General information about Sol-Gel technology: Brief history, sol, gel, gelation concepts, basic concepts in sol-gel processes, current developments, advantages and disadvantages. Chemistry and fundamentals of the Sol-Gel process: Hydrolysis and condensation reactions, types of initiators (silica-based ones, metal oxides), catalysts, electrolytes, aqueous and non-aqueous sol-gel processes; Drying (drying stress, crack-free drying, drying modes (freeze drying, ambient pressure drying, supercritical drying); Characterization methods (structural, chemical, mechanical and biological), Sol-Gel derived materials: Aerogels, synthesis methods, inorganic-silica based aerogels, basic properties and application areas, hydrophobic, superhydrophobic and flexible aerogels; xerogel monoliths, silica ionogels, and ionosilicas, ionic. Obtaining areogel in the presence of liquid, mesoporous ionogels, use of sol-gel materials in pollution management, water treatment, soil reclamation applications, porous gels and membranes, nanocomposite production and characterization methods. : Fundamentals of sol-gel coatings, Biomedical and controlled drug release applications of sol-gel materials.
Weekly Course Content
Week Subject Learning Activities and Teaching Methods
1 The general information on Sol-gel technology and its history Lecturing, Discussion and Q&A
2 The fundementals of sol-gel synthesis and chemistry: hydrolysis and condensation reactions Lecturing, Discussion and Q&A
3 The sol-gel processes with and without water, and catalysts Lecturing, Discussion and Q&A
4 Aging (structural development and mechanical properties) Lecturing, Discussion and Q&A
5 Drying processs and drying types Lecturing, Discussion and Q&A
6 Characterizations (structural and mechanical) Lecturing, Discussion and Q&A
7 Characterizations (chemical and biological) Lecturing, Dscussion and Q&A
8 mid-term exam
9 Sol-gel materials: Aerogels and properties Lecturing, Discussion and Q&A
10 Monolitic sol-gel materials: xerogels Lecturing, Discussion and Q&A
11 silica based ionic gels, mesoporous structures Lecturing, Discussion and Q&A
12 The adsorbent applications of sol-gel materials, porous gels and membranes Lecturing, Discussion and Q&A
13 Nonocomposites, production and characterization methods Lecturing, Discussion and Q&A
14 Thin film coatings Lecturing, Discussion and Q&A
15 Biomedical and drug delivery applications of sol-gel materials Lecturing, Discussion and Q&A
16 final exam
Recommend Course Book / Supplementary Book/Reading
1 1) Innocenzi P., Zub Y.L., Kessler V., G (2007) Sol-Gel Methods for Materials Processing, Springer, The Netherlands
2 Brinker C. J.,Scherer G. W (1990) Sol-Gel Science: The Pyhsics and Chemistry of Sol-Gel Processing, Academic Press Inc., London.
3 Innocenzi P. (2016) The Sol to Gel Transition , Springer, Italy. 4) Koebel M. M, Leventis N. Edts (2011) Aerogel Hadbook, Springer, London.
4 Brinker C.F., Frye G. C., Hurd A.J., Ashley C.S., (1991), Fundamentals of Sol-Gel Dip Coatings, Thin Solid Films, 201, 97-108.
Required Course instruments and materials
Books, Computer, Projector, Online Database, Referencing Software (Mendeley)

Assessment Methods
Type of Assessment Week Hours Weight(%)
mid-term exam 8 1 40
Other assessment methods
1.Oral Examination
2.Quiz
3.Laboratory exam
4.Presentation 12 1 20
5.Report
6.Workshop
7.Performance Project
8.Term Paper 16 2 40
9.Project
final exam

Student Work Load
Type of Work Weekly Hours Number of Weeks Work Load
Weekly Course Hours (Theoretical+Practice) 3 14 42
Outside Class
       a) Reading 3 14 42
       b) Search in internet/Library 3 14 42
       c) Performance Project 0
       d) Prepare a workshop/Presentation/Report 5 2 10
       e) Term paper/Project 4 8 32
Oral Examination 0
Quiz 0
Laboratory exam 0
Own study for mid-term exam 5 4 20
mid-term exam 2 1 2
Own study for final exam 0
final exam 0
0
0
Total work load; 190