Nevşehir Hacı Bektaş Veli University Course Catalogue

Information Of Programmes

ACIGOL VOCATIONAL SCHOOL OF TECHNICAL SCIENCES / LBT203 - LABORATUAR TECHCNOLOGY

Code: LBT203 Course Title: INSTRUMENTAL ANALYSIS Theoretical+Practice: 3+1 ECTS: 4
Year/Semester of Study 2 / Fall Semester
Level of Course Short Cycle Degree Programme
Type of Course Compulsory
Department LABORATUAR TECHCNOLOGY
Pre-requisities and Co-requisites None
Mode of Delivery Face to Face
Teaching Period 14 Weeks
Name of Lecturer ŞEYDA ÇİĞDEM ÖZKAN (seydaozkan@nevsehir.edu.tr)
Name of Lecturer(s)
Language of Instruction Turkish
Work Placement(s) None
Objectives of the Course
To teach the fundamentals of instrumental techniques such as spectroscopic techniques, chromatographic techniques, thermal methods, and analytical applications of instrumental techniques. In addition, the basic principles of modern analysis is to teach.

Learning Outcomes PO MME
The students who succeeded in this course:
LO-1 can classify instrumental analysis techniques. PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically.
Examination
LO-2 Selects the types of techniques required to recognize an unknown sample. PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology.
PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically.
Examination
Laboratory Exam
Presentation
LO-3 Knows the working principles of the devices used in chemistry. PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology.
PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically.
Examination
Laboratory Exam
Presentation
LO-4 Evaluate the experimental data obtained from spectroscopic methods used for the characterization of organic compounds. PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology.
PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically.
Examination
Laboratory Exam
Presentation
LO-5 can apply separation techniques used for the purification of organic compounds. PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology.
PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically.
Examination
Laboratory Exam
Presentation
LO-6 Apply spectroscopic, chromatographic and other analysis techniques. PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology.
PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically.
Examination
Laboratory Exam
Presentation
PO: Programme Outcomes
MME:Method of measurement & Evaluation

Course Contents
Ultraviolet and Visible Spectroscopy (UV-VIS), Infrared Spectroscopy (FT-IR), Nuclear Magnetic Resonance Spectroscopy (NMR), Molecular Luminescence and Chemiluminescence Spectroscopy (Fluorescence and phosphorescence), Mass Spectroscopy (MS), Atomic Spectroscopy, Chromatography Methods Liquid chromatography and its theory; Glass column chromatography; Thin layer chromatography (TLC); Ion exchange chromatography); High performance liquid chromatography (HPLC), Gas chromatography (GC) Polarimetry; Refractometry, Thermal methods (TGA, DTG, DTA).
Weekly Course Content
Week Subject Learning Activities and Teaching Methods
1 Introduction to Instrumental Analysis Lecture, Discussion, Question and Answer
2 UV-Visible Spectroscopy Lecture, Discussion, Question-Answer, Experimentation, Report Preparation
3 IR Spectroscopy Lecture, Discussion, Question and Answer, Experimentation, Report Preparation
4 Nuclear Magnetic Resonance Spectroscopy (NMR) Lecture, Discussion, Question and Answer
5 Nuclear Magnetic Resonance Spectroscopy (NMR) Lecture, Discussion, Question and Answer
6 Nuclear Magnetic Resonance Spectroscopy (NMR) Lecture, Discussion, Question and Answer
7 Mass Spectroscopy Lecture, Discussion, Question and Answer
8 mid-term exam
9 Molecular Luminescence and Chemiluminescence Spectroscopy (Fluorescence and phosphorescence) Lecture, Discussion, Question and Answer
10 Atomic Spectroscopy; AAS and Flame Spectrometers Lecture, Discussion, Question-Answer
11 Chromatography methods (Liquid chromatography and theory; Glass column chromatography; Thin layer chromatography) Lecture, Discussion, Question-Answer, Experimentation, Report Preparation
12 Chromatography methods (Liquid chromatography and theory; Glass column chromatography; Thin layer chromatography) Lecture, Discussion, Question and Answer, Experimentation, Report Preparation
13 Liquid chromatography (LC, LC-MS), Ion exchange chromatography (ICP, ICP-MS Lecture, Discussion, Question and Answer, Experimentation, Report Preparation
14 High performance liquid chromatography (HPLC), chromatography (GC) Lecture, Discussion, Question and Answer, Experimentation, Report Preparation
15 Polarimetry; Refractometry; Electroanalytical Methods; Electrophoretic Methods; Thermal Analysis Methods Lecture, Discussion, Question and Answer, Experimentation, Report Preparation
16 final exam
Recommend Course Book / Supplementary Book/Reading
1 Enstrümental Analiz İlkeleri, Skoog, Holler, Nieman, Bilim Yayıncılık, 5. Baskı
Required Course instruments and materials
Classroom, Projection, Computer, Laboratory and its Equipments

Assessment Methods
Type of Assessment Week Hours Weight(%)
mid-term exam 8 1 20
Other assessment methods
1.Oral Examination
2.Quiz
3.Laboratory exam 4 1 20
4.Presentation
5.Report
6.Workshop
7.Performance Project
8.Term Paper
9.Project
final exam 16 1 60

Student Work Load
Type of Work Weekly Hours Number of Weeks Work Load
Weekly Course Hours (Theoretical+Practice) 4 14 56
Outside Class
       a) Reading 1 14 14
       b) Search in internet/Library 1 14 14
       c) Performance Project 0
       d) Prepare a workshop/Presentation/Report 1 7 7
       e) Term paper/Project 0
Oral Examination 0
Quiz 0
Laboratory exam 1 7 7
Own study for mid-term exam 2 3 6
mid-term exam 1 1 1
Own study for final exam 2 7 14
final exam 1 1 1
0
0
Total work load; 120