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Year/Semester of Study | 2 / Fall Semester | ||||
Level of Course | Short Cycle Degree Programme | ||||
Type of Course | Compulsory | ||||
Department | LABORATUAR TECHCNOLOGY | ||||
Pre-requisities and Co-requisites | None | ||||
Mode of Delivery | Face to Face | ||||
Teaching Period | 14 Weeks | ||||
Name of Lecturer | ŞEYDA ÇİĞDEM ÖZKAN (seydaozkan@nevsehir.edu.tr) | ||||
Name of Lecturer(s) | |||||
Language of Instruction | Turkish | ||||
Work Placement(s) | None | ||||
Objectives of the Course | |||||
To teach the fundamentals of instrumental techniques such as spectroscopic techniques, chromatographic techniques, thermal methods, and analytical applications of instrumental techniques. In addition, the basic principles of modern analysis is to teach. |
Learning Outcomes | PO | MME | |
The students who succeeded in this course: | |||
LO-1 | can classify instrumental analysis techniques. |
PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically. |
Examination |
LO-2 | Selects the types of techniques required to recognize an unknown sample. |
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology. PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field. PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically. |
Examination Laboratory Exam Presentation |
LO-3 | Knows the working principles of the devices used in chemistry. |
PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology. PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field. PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically. |
Examination Laboratory Exam Presentation |
LO-4 | Evaluate the experimental data obtained from spectroscopic methods used for the characterization of organic compounds. |
PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology. PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field. PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically. |
Examination Laboratory Exam Presentation |
LO-5 | can apply separation techniques used for the purification of organic compounds. |
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology. PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field. PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically. |
Examination Laboratory Exam Presentation |
LO-6 | Apply spectroscopic, chromatographic and other analysis techniques. |
PO-1 He/she has theoretical knowledge on basic subjects of chemistry, biology, microbiology and biotechnology.
PO-5 He/she makes basic evaluations in the fields of chemistry, biology, microbiology and biotechnology. PO-6 He/she has the ability to interpret and evaluate data, to identify problems, to analyze and to develop solutions based on evidence, by using the basic knowledge and skills acquired in the field. PO-28 They are knowledgeable about modern and contemporary instrumental analysis techniques, and apply what they have learned effectively and practically. |
Examination Laboratory Exam Presentation |
PO: Programme Outcomes MME:Method of measurement & Evaluation |
Course Contents | ||
Ultraviolet and Visible Spectroscopy (UV-VIS), Infrared Spectroscopy (FT-IR), Nuclear Magnetic Resonance Spectroscopy (NMR), Molecular Luminescence and Chemiluminescence Spectroscopy (Fluorescence and phosphorescence), Mass Spectroscopy (MS), Atomic Spectroscopy, Chromatography Methods Liquid chromatography and its theory; Glass column chromatography; Thin layer chromatography (TLC); Ion exchange chromatography); High performance liquid chromatography (HPLC), Gas chromatography (GC) Polarimetry; Refractometry, Thermal methods (TGA, DTG, DTA). | ||
Weekly Course Content | ||
Week | Subject | Learning Activities and Teaching Methods |
1 | Introduction to Instrumental Analysis | Lecture, Discussion, Question and Answer |
2 | UV-Visible Spectroscopy | Lecture, Discussion, Question-Answer, Experimentation, Report Preparation |
3 | IR Spectroscopy | Lecture, Discussion, Question and Answer, Experimentation, Report Preparation |
4 | Nuclear Magnetic Resonance Spectroscopy (NMR) | Lecture, Discussion, Question and Answer |
5 | Nuclear Magnetic Resonance Spectroscopy (NMR) | Lecture, Discussion, Question and Answer |
6 | Nuclear Magnetic Resonance Spectroscopy (NMR) | Lecture, Discussion, Question and Answer |
7 | Mass Spectroscopy | Lecture, Discussion, Question and Answer |
8 | mid-term exam | |
9 | Molecular Luminescence and Chemiluminescence Spectroscopy (Fluorescence and phosphorescence) | Lecture, Discussion, Question and Answer |
10 | Atomic Spectroscopy; AAS and Flame Spectrometers | Lecture, Discussion, Question-Answer |
11 | Chromatography methods (Liquid chromatography and theory; Glass column chromatography; Thin layer chromatography) | Lecture, Discussion, Question-Answer, Experimentation, Report Preparation |
12 | Chromatography methods (Liquid chromatography and theory; Glass column chromatography; Thin layer chromatography) | Lecture, Discussion, Question and Answer, Experimentation, Report Preparation |
13 | Liquid chromatography (LC, LC-MS), Ion exchange chromatography (ICP, ICP-MS | Lecture, Discussion, Question and Answer, Experimentation, Report Preparation |
14 | High performance liquid chromatography (HPLC), chromatography (GC) | Lecture, Discussion, Question and Answer, Experimentation, Report Preparation |
15 | Polarimetry; Refractometry; Electroanalytical Methods; Electrophoretic Methods; Thermal Analysis Methods | Lecture, Discussion, Question and Answer, Experimentation, Report Preparation |
16 | final exam | |
Recommend Course Book / Supplementary Book/Reading | ||
1 | Enstrümental Analiz İlkeleri, Skoog, Holler, Nieman, Bilim Yayıncılık, 5. Baskı | |
Required Course instruments and materials | ||
Classroom, Projection, Computer, Laboratory and its Equipments |
Assessment Methods | |||
Type of Assessment | Week | Hours | Weight(%) |
mid-term exam | 8 | 1 | 20 |
Other assessment methods | |||
1.Oral Examination | |||
2.Quiz | |||
3.Laboratory exam | 4 | 1 | 20 |
4.Presentation | |||
5.Report | |||
6.Workshop | |||
7.Performance Project | |||
8.Term Paper | |||
9.Project | |||
final exam | 16 | 1 | 60 |
Student Work Load | |||
Type of Work | Weekly Hours | Number of Weeks | Work Load |
Weekly Course Hours (Theoretical+Practice) | 4 | 14 | 56 |
Outside Class | |||
a) Reading | 1 | 14 | 14 |
b) Search in internet/Library | 1 | 14 | 14 |
c) Performance Project | 0 | ||
d) Prepare a workshop/Presentation/Report | 1 | 7 | 7 |
e) Term paper/Project | 0 | ||
Oral Examination | 0 | ||
Quiz | 0 | ||
Laboratory exam | 1 | 7 | 7 |
Own study for mid-term exam | 2 | 3 | 6 |
mid-term exam | 1 | 1 | 1 |
Own study for final exam | 2 | 7 | 14 |
final exam | 1 | 1 | 1 |
0 | |||
0 | |||
Total work load; | 120 |